COMBINED FLOW REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:11, PACKED BED REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:10, ADIBATIC BATCH REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:09, ISOTHERMAL SEMI-BATCH REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:08, ISOTHERMAL BATCH REACTORMAKE : CREATIVE LAB MODEL NO:CLCRE:-07, manufacturers suppliers in India

ISOTHERMAL BATCH REACTORMAKE : CREATIVE LAB MODEL NO:CLCRE:-07

DESCRIPTION:

A batch reactor is a closed system with no input and output streams. A batch reactor can operate under conditions like Isothermal (Temperature of Reaction Mass remains constant), Perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass). This set-up is used to study a non-catalytic homogeneous reaction under isotherCCmal condition. The set up consists of a Reactor fitted in a constant temperature water bath. One stirrer is fitted for mixing the reactants in reactor and other is fitted in water bath to keep the uniform temperature throughout in the bath. The temperature of bath can be maintained from ambient to 90C with the help of Digital Temperature indicator Cum Controller. Samples can be taken out with the help of a sampling pipette.

EXPERIMENTATION:

To study the progress of a Chemicals reaction and determine the kinetic parameters.

To determine the effect of temperature on Reaction Rate Constant.

UTILITY REQUIRED

Water Supply.

Drain.

Electricity Supply: 1 Phase, 220 V AC, 1.5 kW.

Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.

TECHNICAL DETAIL

Reactor Material Stainless Steel, Volume- 1 Ltrs. (Approx.)

Water Bath Material Stainless Steel, Double wall, insulated with Ceramic Wool.

Heater Nichrome wire Heater

Stirrer (2 Nos.) Stainless Steel Impeller and shaft coupled with FHP motor.

Stop Watch Electronic

Temp. Sensor RTD PT-100 type

Control panel comprises of :

Digital Temp. Controller 0-199.9°C, (For Water Bath)

With Standard make on/off switch, Mains Indicator fuses etc.

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

The whole unit is assembled rigidly on a base plate and mounted on a stand.

Most of the parts are powder coated and rest are painted with auto paints.

ISOTHERMAL SEMI-BATCH REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:08

DESCRIPTION:

A isothermal semi-batch reactor is a semi-closed system with one input stream. It is operated under conditions like Isothermal (Temperature of Reaction Mass remains constant) and perfectly mixed (composition of reaction mixture is uniform throughout). This set-up is used to study a non-catalytic homogeneous reaction under isothermal condition. The set up consists of a Reactor fitted in a constant temperature water bath. Before starting the reaction the reactor is charged with measured quantity of one reactant. From a feed tank another reactant is fed to the reactor. Using a sampling pipette samples can be taken out for analysis after fixed interval. Rotameter is provided to measure the flow of Chemicals. The compressed air is used for circulation of feed. One stirrer is fitted for mixing the reactants in reactor and other is fitted in water bath to keep the uniform temperature throughout in the bath. The temperature of bath can be maintained from ambient to 70 ^OC with the help of Digital Temperature indicator Cum Controller. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line.

EXPERIMENTATION:

To study a second order sponification reaction in a Semi-Batch Reactor.

To determine the Reaction Rate Constant.

UTILITY REQUIRED:

Compressed Air Supply at 2 Bar, 0.25 CFM.

Water supply and drain.

Electricity-1.5kw, Single Phase.

Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.

TECHNICAL DETAIL:

Reactor Material Stainless Steel, Capacity 3 Ltrs. (approx.).

Water Bath Material Stainless Steel, Double wall, insulated with Ceramic Wool.

Heater Nichrome wire Heater

Stirrer Material Stainless Steel Impeller and shaft coupled with FHP motor

Feed Tank (1Nos.) Material Stainless Steel, Capacity - 20 Ltrs.

Feed Circulation By compressed air.

Flow Measurement Rotameter.

Piping Material Stainless Steel and PVC.

Pressure Regulator 0-2 Kg/cm2

Pressure Gauge Bourdon type 0-2 Kg/cm2

Stop Watch Electronic

Temp. Sensor RTD PT-100 type

Control panel comprises of :

Digital Temp. Controller 0-199.9°C, RTD PT-100 type (For Water Bath)

With Standard make on/off switch, Mains Indicator etc.

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

The whole unit is assembled rigidly on a base plate and mounted on a stand.

Most of the parts are powder coated and rest are painted with auto paints.

ADIBATIC BATCH REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:09

DESCRIPTION:

An adiabatic batch reactor is a closed system with no input and output streams. This reactor is operated under conditions like adiabatic (Temperature of Reaction Mass keep on changing), perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass). This set-up is used to study a catalytic homogeneous reaction under adiabatic condition. The set-up consists of a Dewar flask of capacity 1 lit. fitted with a stirrer. The flask is double insulated by ceramic wool insulation. Temp. is measured by digital temp indicator. The whole setup is mounted on a rigid M.S. frame.

EXPERIMENTATION:

To study the hydrolysis of acetic anhydride with water in presence of an acid catalyst (H2SO4).

To predict the degree of conversion from time-temperature data.

UTILITY REQUIRED

Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.

TECHNICAL DETAIL

Reactor Material Stainless Steel, Capacity 1 Ltrs. (Approx.)

Insulated with Ceramic wool.

Stirrer Teflon Impeller and Stainless-Steel shaft coupled with FHP motor

Control panel comprises of :

Digital Temp. Indicator 0-199.9°C, RTD PT-100 type

Temp. Sensors RTD PT-100 type

With Standard make on/off switch, Mains Indicator etc.

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

The whole unit is assembled rigidly on a base plate and mounted on a stand.

Most of the parts are powder coated and rest are painted with auto paints.

PACKED BED REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:10

DESCRIPTION:

The setup consists of a glass column packed with Rasching Rings and two feed tanks. Reactants are fed to the reactor through liquid distributor, fitted at the bottom of the column. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. Samples can be taken periodically from the top outlet of reactor. Pressure Regulator & Pressure Gauge are fitted in the compressed air line.

EXPERIMENTATION:

Sponification Reaction studies in Packed Bed Reactor.

To determine the Reaction Rate Constant.

UTILITY REQUIRED:

Compressed Air Supply at 2 Bar, 0.5 CFM.

Water Supply.

Drain.

Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.

TECHNICAL DETAIL:

Reactor Column Material Borosilicate Glass Volume 1.5 Ltrs. (approx).

Packing Rasching Rings, Material Borosilicate Glass.

Size 6-8 mm (approx)

Feed Tank (2Nos.) Material Stainless Steel, Capacity - 20 Ltrs..

Feed Circulation By compressed air.

Flow Measurement Rotameter 2Nos. (one each for Reactants).

Piping Stainless Steel and PVC.

Pressure Regulator 0-2 Kg/cm2

Pressure Gauge Bourdon type 0-2 Kg/cm2

Stop Watch Electronic.

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

The whole unit is assembled rigidly on a Panel plate and mounted on a stand.

Most of the parts are powder coated and rest is painted with auto paints.

COMBINED FLOW REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:11

DESCRIPTION:

This set-up is used to study a non-catalytic homogeneous second order liquid phase reaction under ambient condition in a combined reactor. It consists of two reactors connected in series, one is plug flow reactor and another mixed flow reactor. In an ideal Plug Flow Reactor (PFTR) there is no mixing in the direction of flow and complete mixing perpendicular to direction of flow. Concentration of reactants varies along the length of reactor but not in radial direction. In case of a coil turbulence is introduced due to frequent change in direction of flow and presence of secondary flow, so a higher value of reaction rate constant is expected in coil tube type plug flow reactor. In an ideal MFR (i.e. an ideal steady state flow reactor) the contents in reactor are well mixed and have uniform composition throughout. Thus the exit stream has the same composition as the fluid within the reactor. The set up consists of two feed tanks through which two reactants are fed to the reactors fitted in series. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on respective Rotameter. The compressed air is used for circulation of feed. 1st is a helical coil tube type reactor made up of SS pipe. Reactants enter at lower end coming out of the top of coil from where it is fed to a MFR fitted with stirrer for proper mixing. Samples are collected for analysis. Pressure Regulator, Pressure Gauge and Safety Valve are fitted in the compressed air line. The same setup can be used as individual Plug Flow Reactor (Coil Tube type) and Mixed Flow Reactor.

EXPERIMENTATION:

Sponification Reaction Study in a Combined Reactor

Sponification Reaction Study in Coil Tube Type Plug Flow Reactor

Sponification Reaction Study in a MFR.

To determine Reaction Rate Constant.

UTILITY REQUIRED:

Compressed Air Supply at 1 HP, 2 CFM.

Water Supply.

Drain.

Electricity Supply: 1 Phase, 220 V AC, 0.5 kW.

Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted.

TECHNICAL DETAIL:

1st Reactor Material Stainless Steel, Capacity 0.7 Ltrs. (approx) (Helical Coiled tube type)

2nd Reactor Material Stainless Steel, Capacity 2 Ltrs (Approx).

Stirrer for MFR Stainless Steel Impeller and shaft coupled with FHP motor Standard make.

Feed Tank (2Nos.) Material Stainless Steel, Capacity - 20 Ltrs.

Feed circulation By compressed air.

Flow Measurement Rotameter 2 Nos. (one each for Reactants) Eureka/IEPL make.

Piping Stainless Steel and PVC

Pressure Regulator 0-2 Kg/cm2 Janetics/Shavo Norgen make.

Pressure Gauge Bourdon type 0-2 Kg/cm2 Mass/Pricol make.

Stop Watch Electronic.

Instruction Manual An ENGLISH instruction manual will be provided along with the Apparatus

The whole unit is assembled rigidly on a base plate and mounted on a stand.

Most of the parts are powder coated and rests are painted with auto paints.

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COMBINED FLOW REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:11 PACKED BED REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:10 ADIBATIC BATCH REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:09 ISOTHERMAL SEMI-BATCH REACTOR MAKE : CREATIVE LAB MODEL NO:CLCRE:08 ISOTHERMAL BATCH REACTORMAKE : CREATIVE LAB MODEL NO:CLCRE:-07